USP Solvents
Method: | GC |
Matrix: | Standards |
Application No.: | 101151 |
Columns: | DM-1 60 m x 0.53 mm x 3.00 μm |
Cat No.: | 7156 |
Conditions: | Oven Temp.: 35 ºC (hold 4min) to 250 ºC at 4 ºC/min septa purge 5 mL/min Carrier Gas: He, 45.6 cm/sec, 35 ºC Head Pressure: 11.0 psi constant pressune Injection: Split, 100 mL/min, ~1:13, 250 ºC Sample: Solvents, ~1.3% each Detector: MS Scan Range: 10 AMU - 260 AMU |
Author: | Dikma Technologies Inc. |
Publisher: | CER00463 |
Keyword: | USP, Residual solvent, solvent residue, pharmacy, GC, DM-1, EPA |
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Table: | 1. Formaldehyde 2. Water 3. Chloromethane 4. Methanol 5. Acetaldehyde 6. Ethylene oxide 7. Chloroethane 8. Ethanol 9. Acetonitrile 10. Acetone 11. 2-Propanol 12. 2-Chloropropane 13. Diethyl ether 14. Pentane 15. Ethyl formate 16. Formic acid 17. Methylal 18. 1,1-Dichloroethene 19. Methyl acetate 20. Methylene chloride 21. Nitromethane 22. 1-Propanol 23. trans -1,2-Dichloroethene 24. Methyl tert -butyl ether 25. 2-Methylpentane (spiked at 9%) 26. 2-Butanone 27. 2-Butanol 28. cis -1,2-Dichloroethene 29. Acetic acid 30. Isopropyl ether 31. Ethyl acetate 32. Hexane 33. Chloroform 34. Tetrahydrofuran 35. 2-Methoxyethanol 36. 1,2-Dichloroethane 37. Methyl cyclopentane 38. 1,1,1-Trichloroethane 39. 1,2-Dimethoxyethane 40. Methyl isopropyl ketone 41. 2,2-Dimethoxypropane 42. Isopropyl acetate 43. 1-Butanol 44. Benzene 45. Carbon tetrachloride 46. Ethylene glycol 47. Formamide 48. 1,4-Dioxane 49. Trichloroethylene 50. Isooctane 51. 2-Ethoxyethanol 52. n-Heptane 53. Isoamyl alcohol 54. Hexanone 55. Pyridine 56. Methyl cyclohexane 57. Dimethyl formamide 58. 1,1,2-Trichloroethane 59. 1-Pentanol 60. Isobutyl acetate 61. Toluene 62. 2-Hexanone 63. Dimethyl sulfoxide 64. Butyl acetate 65. 1,1-Diethoxypropane 66. N,N-Dimethylacetamide 67. Chlorobenzene 68. Ethylbenzene 69. Isoamyl acetate 70. p-Xylene 71. m-Xylene 72. o-Xylene 73. Anisole 74. Isopropyl benzene (Cumene) 75. 1-Methyl-2-pyrrolidinone 76. Sulfolane 77. 1,2,3,4-Tetrahydronaphthalene |
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